Jan. 26: Introduction. Kinetics: Solvolysis of t-Butyl Chloride (Manual Exp. 1)
Feb. 2: Kinetics (cont.). Friedel-Crafts Alkylation (Manual Exp. 2)
Feb. 9: Friedel-Crafts (cont.)/GC. Intro. to NBS Bromination (Manual Exp. 3)
Feb. 16: NBS/NMR (cont.). Intro. to Diels-Alder (Manual Exp. 4)
Feb. 23: Diels-Alder (cont.). Esterification (Manual Exp. 5)
March 2: Esterification (cont.). Grignard Reactions
March 9 : Grignard/TLC (cont.)
March 16 : Practice (your questions). Introduction to Unknowns
MIDTERM in your lab, 2:10 - 4 pm; BRING CALCULATOR!
March 23 : Unknowns: Solubility tests. Classification tests. Derivatives.
Use Chapter 10 in your lab textbook for analytical procedures.
Below are two additional procedures:
SPRING BREAK
April 6 : Cont. Unknowns
April 13: Conclusion Unknowns. UV
April 20: IR
April 27 : Mass Spectrometry Bring your Unknown #3 spectra to Lab Lecture if you have them!
May 4: H-NMR and CMR Bring your Unknown #3 spectra!
May 11: Your questions
FINAL EXAM in your lab 2:10 pm